Ethyl vanillin was synthesized by the phase-transfer catalysis CTEAB and O-ethoxyphenol, which was prepared from pyroeat摘要以邻苯二酚为原料，首先合成中间体邻乙氧基苯酚，然后以十六烷基三乙基溴化铵为相转移催化剂合成了乙基香兰素，考察了相转移催化剂的选择及反应温度，最后收率为55.2%。