Five diacylthiourea compounds were synthesized by his (trichloromethyl) carbonate (BTC). The production structures were confirmed by elemental analysis, IR. The yield and purity of the products were 85.6%~91.8% and 96.5%~97.9%, respectively.
Five diacylthiourea compounds were synthesized by his (trichloromethyl) carbonate (BTC). The production structures were confirmed by elemental analysis, IR. The yield and purity of the products were 85.6%~91.8% and 96.5%~97.9%, respectively.
摘要用二（三氯甲基）碳酸酯(BTC)代替光气，“一锅法”合成了5种双酰基硫脲化合物，产物结构经元素分析、IR确证。收率为85.6%~91.8%、纯度为96.5%~97.9%。