The paper introduces a new highly-effective synthesis method. Decoquinate was synthesized with catechol as starting materials via substitution, reduction, and at last cyclization with Dowtherm Aas solvent.
The paper introduces a new highly-effective synthesis method. Decoquinate was synthesized with catechol as starting materials via substitution, reduction, and at last cyclization with Dowtherm Aas solvent.
摘要以邻苯二酚为原料，通过一系列取代反应，再经过还原、缩合，最后在高沸点的混合有机溶剂中关环。制备的3-喹啉羧酸乙酯衍生物的总收率为24.2%。