The novel title compound was synthesized with benzaldehyde, isobutyraldehyde, phosphorus trichloride as raw materials. The total yield was 40.8%. The structure was confirmed by 1H NMR, 31P NMR and elemental analysis.
The novel title compound was synthesized with benzaldehyde, isobutyraldehyde, phosphorus trichloride as raw materials. The total yield was 40.8%. The structure was confirmed by 1H NMR, 31P NMR and elemental analysis.
摘要以苯甲醛、异丁醛、三氯化磷为原料合成了新型的1,3,2-氧磷杂环类化合物2-苯羟甲基－5,5-二甲基－4-苯基－2-氧代－1,3,2-二氧磷杂环己烷，总收率为40.8%，并对其进行了NMR研究和结构表征。