The chromatographic conditions are as fellows:ODS-AM- 0 column(YMC,.mm×0mm,μm)with the temperature of 0℃,acetonitrile-water(0∶0)containing 0.% trifluo roacetic acid as mobile phase with the flow rate of mL/min.
The chromatographic conditions are as fellows:ODS-AM- 0 column(YMC,.mm×0mm,μm)with the temperature of 0℃,acetonitrile-water(0∶0)containing 0.% trifluo roacetic acid as mobile phase with the flow rate of mL/min.
色谱条件为:ODS-AM- 0 色谱柱(YMC,.mm×0mm,μm),柱温0℃,含0.%三氟乙酸的乙腈-水(0∶0)为流动相,流速mL/min。