u-Oxo bis [tetraphenylporphinatoiron (Ⅲ)], [TPPFe (Ⅲ)]_O, was synthesized by passing chloro [tetraphenylporphinatoiron (Ⅲ)], TPPFe(Ⅲ)Cl, through a neutral Al_O_ chromatographic column, and was characterized by HPLC, IR, UV-Vis and elemental analysis.
u-Oxo bis [tetraphenylporphinatoiron (Ⅲ)], [TPPFe (Ⅲ)]_O, was synthesized by passing chloro [tetraphenylporphinatoiron (Ⅲ)], TPPFe(Ⅲ)Cl, through a neutral Al_O_ chromatographic column, and was characterized by HPLC, IR, UV-Vis and elemental analysis.
TPPFe(Ⅲ)Cl通过中性Al_O_ 色谱柱得到一个新化合物,它在HPLC中的保留时间比TPPFe(Ⅲ)Cl大得多,IR、UV-Vis和元素分析表明,这个新化合物是[TPPFe(Ⅲ)]_~O.